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The cell suspension was spun down at 14,000 g for 10 minutes, and 3 µl of supernatant was applied to an Accucore 150 Amide HILIC HPLC column (100 × 2.1 mm, 2.6-µm particle size) equipped with a guard cartridge (at 30 °C)

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doi: 10.1186/s13024-020-00388-2, PMID: [DOI] [PMC free article] [PubMed] [Google Scholar] Vance J